Solid phase microextraction (SPME) in determination of pesticide residues in soil samples
نویسندگان
چکیده
منابع مشابه
Optimization of headspace solid-phase microextraction for the determination of pesticide residues in vegetables and fruits.
A headspace solid-phase microextraction method has been developed for the determination of 8 pesticides in vegetables and fruits by using gas chromatography with an electron capture detector. Two types of fibers (polyacrylate, 85 microm and polydimethylsiloxane, 100 microm) have been assayed and compared. The main factors: extraction and desorption parameters, ionic strength, and the effects of...
متن کاملSolid-phase microextraction for herbicide determination in environmental samples.
Liquid-liquid extraction or solid-phase extraction followed by gas chromatography (GC) or high-performance liquid chromatography are traditional herbicide residue determination methods for environmental samples. Solid-phase microextraction (SPME) is a solventless, fast, and sensitive alternative herbicide residue extraction method that can be applied to numerous environmental matrices. The obje...
متن کاملHCl- Etched Steel Fiber for Determination of Phthalates in Water Samples by Solid-Phase Microextraction
In the present work, a stainless steel wire was etched by hydrochloric acid during a chemical etching process. The obtained black layer on the surface of the fiber was used as sorbent for extraction of trace amount of phthalates in the aqueous samples by solid phase microextraction. New fiber efficiency was investigated using a home-made solid-phase microextraction (SPME) device and gas chr...
متن کاملSolid-phase microextraction and headspace solid-phase microextraction for the determination of polychlorinated biphenyls in water samples.
A solid-phase microextraction (SPME) method has been developed for the quantification of polychlorinated biphenyls (PCBs) in water samples. Parameters such as sampling time, volume of water, volume of headspace, temperature, addition of salts, and agitation of the sample were studied. Because the time for reaching equilibrium between phases takes several hours or days, depending on the experime...
متن کاملapplication of solid phase microextraction (spme) sampler for determination of carbon disulfide in air
carbon disulfide is used predominantly in the manufacture. it has affects the nervous system. in this study, the applicability of spme as a passive sampler for determination of carbon disulphide in air was studied. effect of sampler and environmental parameters on uptake of carbon disulphide was studied as well. four fibers were tested to select the best sampler for determine carbon disulfide i...
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ژورنال
عنوان ژورنال: Pesticidi i fitomedicina
سال: 2011
ISSN: 1820-3949,2406-1026
DOI: 10.2298/pif1103177d